Operation of the hydrothermal synthesis digestion tank.
1.Pour the reaction material into the PTFE bushing (temperature resistant to 200 degrees) or PPL para-polyphenyl bushing (temperature resistant to 280 degrees) and ensure that the filling factor is less than 0.8.
2.Make sure that the lower gasket of the kettle is correctly positioned (raised side down), then put in the PTFE bushing or PPL bushing and the upper gasket, tighten the kettle cover first, and then screw the kettle cover until it is twisted and tightened with a screw.
3.Place the hydrothermal kettle in the heater and raise the temperature to the required reaction temperature according to the specified heating rate. (less than the specified safe operating temperature).
4.Only open the lid of the kettle when it has been confirmed that the temperature inside the belly is below the boiling point of the solvent of the reactant species. When the reaction is finished and the temperature is cooled down, it is also necessary to strictly follow the prescribed cooling rate in order to ensure safety and the service life of the reactor.
5.After confirming that the temperature inside the belly is lower than the boiling point of the solvent of the reactant, first loosen the lid with the screw and then open the lid.
6.Clean the kettle in time after each use to avoid rust and corrosion. Take extra care to clean the sealing area of the kettle body and lid, and prevent them from being damaged by bruising.
1. Good corrosion resistance, resistant to strong acids and alkalis, no spillage of harmful substances, environmentally safe.
2. Under certain conditions of temperature and pressure, it can quickly dissolve samples that are difficult to dissolve at room temperature and samples containing volatile elements without damage.
3. Beautiful and light appearance, simple results, easy to operate and understand.
4. Shortened reaction time, stable reaction results and reliable data.
| Products Name |
Hydrothermal Synthesis Reactor |
| Working temperature |
≤220ºC |
| Working pressure |
3MPa |
| Heating and cooling rate |
≤5ºC/min |
| Reaction volume |
10ML/20ml/25ml/50ml/100ml/200ml/500ml/1000ml/2000ml |
| Chamber Material |
High quality PTFE |
| The outer material is high quality stainless steel, the inner material is ptfe. The hydrothermal synthesis reactor is sealed with circular tenon groove, and the sealing effect can be achieved by manual screw to ensure long-term sealing without leakage. |
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